Proceedings of the 2016 International Forum on Mechanical, Control and Automation (IFMCA 2016)

Comparision and evaluation of two pretreatments of different mechanisms for multi-Fusarium toxins

Authors
Jia-Ning Zhang, Ke Ding, Xiang-Ning Chen, Tao Han
Corresponding Author
Jia-Ning Zhang
Available Online March 2017.
DOI
https://doi.org/10.2991/ifmca-16.2017.134How to use a DOI?
Keywords
Immunoaffinity columns, MycoSep®226 multifunction purifying columns, Fusarium toxins, flour , liquid chromatography mass spectrometryzz (LC-MS/MS)
Abstract
A simultaneous determination method for four kinds of Fusarium toxins (zearalenone, deoxynivalenol, T-2 and HT-2 toxins) in flour was established using high performance liquid chromatography-tendem mass spectrometry (LC-MS/MS). Samples were cleaned up with MycoSep®226 multifunction purifying columns and immunoaffinity columns DZT MS-PREP separately. The recovery of the Mycosep® 226 multifunction purifying column is 69.42%~111.12%, and the relative standard deviation is 1.46%~13.24%. The recovery of the immunoaffinity columns DZT MS-PREP is 88.01%~107.31%, and the relative standard deviation is 1.09%~14.42%. 7 kinds of flour samples were determined, most of the detection results of the immunoaffinity columns DZT MS-PREP were higher than that of the Mycosep® 226 multifunction purifying column. The immunoaffinity columns provides an alternative effective and fast tool for simultaneous extraction of the residues of four Fusariumtoxins from real samples.
Open Access
This is an open access article distributed under the CC BY-NC license.

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Volume Title
Proceedings of the 2016 International Forum on Mechanical, Control and Automation (IFMCA 2016)
Series
Advances in Engineering Research
Publication Date
March 2017
ISBN
978-94-6252-307-4
ISSN
2352-5401
DOI
https://doi.org/10.2991/ifmca-16.2017.134How to use a DOI?
Open Access
This is an open access article distributed under the CC BY-NC license.

Cite this article

TY  - CONF
AU  - Jia-Ning Zhang
AU  - Ke Ding
AU  - Xiang-Ning Chen
AU  - Tao Han
PY  - 2017/03
DA  - 2017/03
TI  - Comparision and evaluation of two pretreatments of different mechanisms for multi-Fusarium toxins
BT  - Proceedings of the 2016 International Forum on Mechanical, Control and Automation (IFMCA 2016)
PB  - Atlantis Press
SP  - 855
EP  - 863
SN  - 2352-5401
UR  - https://doi.org/10.2991/ifmca-16.2017.134
DO  - https://doi.org/10.2991/ifmca-16.2017.134
ID  - Zhang2017/03
ER  -