Tow Solid-state 13C Nuclear Magnetic Resonance Methods for Detecting Chemical Structure of Coal Combustion Emissions
Authors
Xiangyun Zhang, Jun Li, Yangzhi Mo, Gan Zhang
Corresponding Author
Xiangyun Zhang
Available Online December 2016.
- DOI
- 10.2991/icseee-16.2016.106How to use a DOI?
- Keywords
- Nuclear Magnetic Resonance; Coal combustion emissions; CP-TOSS/MAS; DP/MAS; Component analysis.
- Abstract
This work introduces tow solid-state 13C Nuclear Magnetic Resonance(NMR) methods, cross polarization- total suppression of sidebands/magic angle spinning (CP-TOSS/MAS) and direct polarization/magic angle spinning (DP/MAS), for detecting chemical structure of coal combustion emissions. The CP-TOSS/MAS NMR experiment result of the standard sample overestimate the value of sp3-C group (25±5%). This is also demonstrated in the Pingdingshan coal combustion emissions sample. DP/MAS NMR is more accurate in detecting the structure of compounds, but this method need much more time.
- Copyright
- © 2016, the Authors. Published by Atlantis Press.
- Open Access
- This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).
Cite this article
TY - CONF AU - Xiangyun Zhang AU - Jun Li AU - Yangzhi Mo AU - Gan Zhang PY - 2016/12 DA - 2016/12 TI - Tow Solid-state 13C Nuclear Magnetic Resonance Methods for Detecting Chemical Structure of Coal Combustion Emissions BT - Proceedings of the 2016 5th International Conference on Sustainable Energy and Environment Engineering (ICSEEE 2016) PB - Atlantis Press SP - 583 EP - 586 SN - 2352-5401 UR - https://doi.org/10.2991/icseee-16.2016.106 DO - 10.2991/icseee-16.2016.106 ID - Zhang2016/12 ER -