Proceedings of the 3rd KOBI Congress, International and National Conferences (KOBICINC 2020)

Synthesis of Mesoporous Silica From Beach Sand Using Variation of Cetyl Trimethyl Ammonium Bromide (CTAB)

Authors
Lisna Efiyanti, Wega Trisunaryanti, Syaiful Bahri, Yatim Lailun Ni’mah, Nia Meisa Wulandari, Satriyo D. Sumbogo
Corresponding Author
Lisna Efiyanti
Available Online 23 June 2021.
DOI
10.2991/absr.k.210621.063How to use a DOI?
Keywords
beach sand, CTAB, mesoporous, silica
Abstract

The potential for sand in Indonesia is very abundant because Indonesia has a long coastline than other countries. This research was conducted to explore the potential of beach sand as an alternative raw material to replace commercial silica. To obtain the natural silica, the beach sand was prepared and extracted into mesoporous silica. The reflux method was chosen to extract silica using NaOH solution, HCl solution, and CTAB surfactant. The mesoporous structure was potentially affected by CTAB and SiO2 ratio, and therefore, this research was focused more on the effect of CTAB weight variation (3; 4,5 and 6 g). Several instruments were used to analyze the characteristics of silica, such as Surface Area Analyzer (SAA), Scanning Electron Microscopy (SEM), and Fourier Transform Infrared Spectroscopy (FTIR). The mesoporous silica has siloxane (Si-O-Si) and silanol (Si-OH) functional group and showed a coral reef-like structure. The porosity properties of these materials ranging from 300-385 m2/g for the specific surface area, 5-8.8 nanometer for pore diameter, and 0.4-0.8 cm3/g for pore volume. Optimal CTAB weight found to be at 6 g, which produces the mesoporous silica with a surface area of 385.928 m2/g, an average pore diameter of 6.015 nanometers, and pore volume of 0.579 cm3/g.

Copyright
© 2021, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

Download article (PDF)

Volume Title
Proceedings of the 3rd KOBI Congress, International and National Conferences (KOBICINC 2020)
Series
Advances in Biological Sciences Research
Publication Date
23 June 2021
ISBN
978-94-6239-399-8
ISSN
2468-5747
DOI
10.2991/absr.k.210621.063How to use a DOI?
Copyright
© 2021, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

Cite this article

TY  - CONF
AU  - Lisna Efiyanti
AU  - Wega Trisunaryanti
AU  - Syaiful Bahri
AU  - Yatim Lailun Ni’mah
AU  - Nia Meisa Wulandari
AU  - Satriyo D. Sumbogo
PY  - 2021
DA  - 2021/06/23
TI  - Synthesis of Mesoporous Silica From Beach Sand Using Variation of Cetyl Trimethyl Ammonium Bromide (CTAB)
BT  - Proceedings of the 3rd KOBI Congress, International and National Conferences (KOBICINC 2020)
PB  - Atlantis Press
SP  - 374
EP  - 381
SN  - 2468-5747
UR  - https://doi.org/10.2991/absr.k.210621.063
DO  - 10.2991/absr.k.210621.063
ID  - Efiyanti2021
ER  -