The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid

DOI

10.2991/ifeesd-16.2016.142How to use a DOI?

Keywords

2,3-dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid, organic light-emmitting material, synthesis, -conjugated polymers

Abstract

A new synthetic approach to synthesize 2,3-dimethyl -2,3-dihydrofuro [3,4-b][1,4] dioxine-5,7 -dicarboxylic acid from a common precursor diglycolic acid was reported. Starting from the commercial material diethylene glycol, diethyl oxalate and 2,3-dibromobutane, the compound was synthesized through oxidation reaction, acylation, hydrolysis and elimination reaction with moderate yield via a five-step reaction. The procedure was described herein with several advantages, including high product yields and easy purification.

Copyright

© 2016, the Authors. Published by Atlantis Press.

Open Access

This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

Download article (PDF)

TY  - CONF
AU  - Liping Wang
AU  - Diandian Deng
AU  - Hewei Yan
AU  - Xiaoxia Sun
AU  - Chaochao Wei
PY  - 2016/05
DA  - 2016/05
TI  - The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid
BT  - Proceedings of the 2016 International Forum on Energy, Environment and Sustainable Development
PB  - Atlantis Press
SP  - 776
EP  - 779
SN  - 2352-5401
UR  - https://doi.org/10.2991/ifeesd-16.2016.142
DO  - 10.2991/ifeesd-16.2016.142
ID  - Wang2016/05
ER  -