Synthesis and Characterization of (-)-Dibornyl Oxalate
- https://doi.org/10.2991/ic3me-15.2015.86How to use a DOI?
- (-)-Borneol, Oxalyl Chloride, (-)-Dibornyl oxalate, Characterization
(-)-Dibornyl oxalate was synthesized by the reaction of natural (-)-borneol with oxalyl chloride under the optimized reaction conditions: temperature 35 , time 1 h and the molar ratio of (-)-borneol and oxalyl chloride 1.0 : 0.6. The reaction underwent in good selectivity as 99 % for target product which can be easily purified to 99.9 % through recrystallization. The structure of (-)-dibornyl oxalate was characterized by GC-MS, FT-IR, 1H NMR and 13C NMR.
- © 2015, the Authors. Published by Atlantis Press.
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Cite this article
TY - CONF AU - Xiaomin Yuan AU - Zhendong Zhao AU - Shichao Xu AU - Yuxiang Chen AU - Liangwu Bi PY - 2015/08 DA - 2015/08 TI - Synthesis and Characterization of (-)-Dibornyl Oxalate BT - Proceedings of the 3rd International Conference on Material, Mechanical and Manufacturing Engineering PB - Atlantis Press SP - 437 EP - 440 SN - 2352-5401 UR - https://doi.org/10.2991/ic3me-15.2015.86 DO - https://doi.org/10.2991/ic3me-15.2015.86 ID - Yuan2015/08 ER -